Title:	Determinação de resíduos de pesticidas em plasma bovino por cromatografia gasosa-espectrometria de massas.
Authors:	MAFFEI, D. F. NOGUEIRA, A. R. de A. BRONDI, S. H. G.
Affiliation:	DANIELE FERNANDA MAFFEI, UNICEP, SÃO CARLOS, SP.; ANA RITA DE ARAUJO NOGUEIRA, CPPSE; SILVIA HELENA GOVONI BRONDI.
Date Issued:	2009
Citation:	Química Nova, v. 32, n. 7, p. 1713- 716, 2009.
Description:	An analytical method for the isolation based on matrix solid-phase dispersion technique and gas chromatographic determination of pesticides in cattle plasma is presented. It was fortified 0.25 g of plasma with pesticides and blended with 1 g each C18 and Na2SO4. The homogenized matter was transferred to a SPE cartridge, which contained 1 g of activated florisil with 5 mL acetonitrile. The analites were eluted under vaccum with 15 mL acetonitrile, the extract was analyzed by gas chromatography-mass spectrometry. The limit of quantification of the method was 0.04 mg L-1 for chlorphenvinfos and fipronil and 0.02 mg L-1 for cypermethrin.
Thesagro:	Residuo Pesticida Plasma Bovino
Keywords:	MSPD GC MS
DOI:	https://doi.org/10.1590/S0100-40422009000700006
Type of Material:	Artigo de periódico
Access:	openAccess
Appears in Collections:	Artigo em periódico indexado (CPPSE)