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dc.contributor.authorNOGUEIRA, A. R. de A.por
dc.contributor.authorARAÚJO, G. C. L.por
dc.contributor.authorNÓBREGA, J. A.por
dc.contributor.otherANA RITA DE ARAUJO NOGUEIRA, CPPSE.por
dc.date.accessioned2015-02-21T09:40:32Z-
dc.date.available2015-02-21T09:40:32Z-
dc.date.created2000-04-20por
dc.date.issued2000por
dc.identifier.other12685por
dc.identifier.urihttp://www.alice.cnptia.embrapa.br/alice/handle/doc/44768por
dc.descriptionMicrawave decomposition has been increasingly used hr a large number of samples. A method using an open vessel microwave was used for biological sample preparation with nitric acid vapors under atmospheric pressure. A lab made Teflon@ support suited with four cups, which received the samples, was inserted in the microwave vessel. These cups were used to weight 30 mg of certi5ed re5wence materials such as spinach and apple leaves, which received 150 pL of d.i. water to improve the micrawave e%ciency. This mixture was exposed to acid vapor stemmed from 15 mL of concentrated nitrie acid plsced in the bottom of the vessel hr decompoeition. The maximum microwave temperature, 115'C, was reached in 4 min. This condition was rnaintained hr 20 min to sllow complete decomposition of the sample. The deeomposed sample, in the cup, was diluted to 1.0 mL of d.i. water, shaken and centrifuged. The cups were than placed directed into an autosampler for Co and Fe analysis in an atomic absorption graphite fumace spectrometer.por
dc.description.uribitstream/item/118360/1/digitalizar0004.pdfpor
dc.languagept_BRpor
dc.language.isoporpor
dc.publisherIn: PITTCON, 21., 2000, New Orleans. Abstracts... New Orleans: PITTCON,2000.por
dc.relation.ispartofEmbrapa Pecuária Sudeste - Artigo em anais de congresso (ALICE)por
dc.rightsopenAccesspor
dc.subjectMicrovawepor
dc.subjectDecompostionpor
dc.subjectAcid vaporpor
dc.subjectOpen vessel.por
dc.titleAcid vapor sample decomposition in open vessel microwave.por
dc.typeArtigo em anais de congresso (ALICE)por
dc.date.updated2015-02-21T09:40:32Zpor
dc.subject.nalthesauruscobalt.por
dc.ainfo.id44768por
dc.ainfo.lastupdate2015-02-20por
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