Please use this identifier to cite or link to this item: http://www.alice.cnptia.embrapa.br/alice/handle/doc/960760
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dc.contributor.authorBRONDI, S. H. G.
dc.contributor.authorSOUZA, G. B. de
dc.contributor.authorNOGUEIRA, A. R. de A.
dc.contributor.authorCAMARGO, L. A. DE
dc.contributor.authorMAJARON, R. F.
dc.date.accessioned2023-05-15T10:47:45Z-
dc.date.available2023-05-15T10:47:45Z-
dc.date.created2013-06-27
dc.date.issued2013
dc.identifier.citationQuímica Nova, v. 36, n. 1, p. 153-158, 2013.
dc.identifier.urihttp://www.alice.cnptia.embrapa.br/alice/handle/doc/960760-
dc.descriptionAnalytical methods were developed and validated to determine residues of veterinary drugs in buffalo milk and meat, using the QuEChERS method and gas chromatography-mass spectrometry. Both milk and meat, at 2 g of sample, 4 mL of acetonitrile, 0.8 g of MgSO4 and 0.2 g of NaCl, were used in the liquid-liquid partition, whereas 50 mg of C18, 50 mg of PSA and 150 mg of MgSO4 were employed in the dispersive solid-phase extraction (d-SPE). The methods showed sensitivity, precision and accuracy. The quantitation limits were in agreement with the maximum residue limit established by the Codex Alimentarius, FAO and WHO.
dc.language.isopor
dc.rightsopenAccess
dc.subjectCG EM
dc.subjectQuEChERS method
dc.subjectVeterinary drug
dc.titleDesenvolvimento e validação do método QuEChERS na determinação de resíduos de medicamentos veterinários em leite e carne de búfalo.
dc.typeArtigo de periódico
riaa.ainfo.id960760
riaa.ainfo.lastupdate2023-05-12
dc.identifier.doihttps://doi.org/10.1590/S0100-40422013000100025
dc.contributor.institutionSILVIA H. G. BRONDI; GILBERTO BATISTA DE SOUZA, CPPSE; ANA RITA DE ARAUJO NOGUEIRA, CPPSE; LAÍS A. DE CAMARGO, Universidade Federal de São Carlos; RAFAELA F. MAJARON, Universidade Federal de São Carlos.
Appears in Collections:Artigo em periódico indexado (CPPSE)

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