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Title: | An NMR tool for cyclodextrin selection in enantiomeric resolution by high-performance liquid chromatography. |
Authors: | LAVERDE JÚNIOR, A. CONCEIÇÃO, G. J. A. da QUEIROZ, S. C. do N. de FUJIWARA, F. Y. MARSAIOLI, A. J. |
Affiliation: | A. LAVERDE JÚNIOR, IQ/Unicamp; G. J. A. da CONCEIÇÃO, IQ/Unicamp; SONIA CLAUDIA DO N DE QUEIROZ, CNPMA; F. Y. FUJIWARA, IQ/Unicamp; A. J. MARSAIOLI, IQ/Unicamp. |
Date Issued: | 2002 |
Citation: | Magnetic Ressonance in Chemistry, Chichester, v. 40, p. 433-442, 2002. |
Description: | Complexation-induced chemical shifts and diffusion coefficients (HR-DOSY) of enantiomers with native and derivatized cyclodextrins were used for calculations of the apparent binding constants of three cyclohexanone inclusion complexes. Correlations between these data and high-performance liquid chromatography were established, revealing that this approach can be applied as an alternative method to predict enantiomeric discrimination. |
Thesagro: | Cromatografia Análise química |
Type of Material: | Artigo de periódico |
Access: | openAccess |
Appears in Collections: | Artigo em periódico indexado (CNPMA) |
Files in This Item:
File | Size | Format | |
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LaverdeNMR6426.pdf | 208,91 kB | Adobe PDF | View/Open |