Title:	High enhancement of macro and micronutrients quantification in Cajuína by ICP OES using ultrasound and multivariate analysis.
Authors:	COELHO, T. L. S. SILVA, D. S. N. SOUZA FILHO, L. B. DE ROCHA, J. M. MARCANO DE HIGUERA, J. SÁ, I. P. DE GAMELA, R. R. NOGUEIRA, A. R. de A. LOPES JÚNIOR, C. A. VIEIRA, E. C.
Affiliation:	TIAGO LINUS SILVA COELHO, Federal University of Piauí; DARLISSON SLAG NERI SILVA, Federal University of Piauí; LUIZ BRITO DE SOUZA FILHO, Federal University of Piauí; JARDEL MENEZES ROCHA, Federal University of Piauí; JULYMAR MARCANO DE HIGUERA, Federal University of São Carlos; IVERO PITA DE SÁ, Federal University of São Carlos; RAIMUNDO RAFAEL GAMELA, Higher Polytechnic Institute of Gaza; ANA RITA DE ARAUJO NOGUEIRA, CPPSE; CÍCERO ALVES LOPES JÚNIOR, Federal University of Piauí; EDIVAN CARVALHO VIEIRA, Federal University of Piauí.
Date Issued:	2023
Citation:	Food Chemistry Advances, v. 2, 2023.
Pages:	8 p.
Description:	A fast, safe, simple, and low-cost analytical method was developed for the determination of macro and microelements in Cajuína samples from Brazil combining UAE and ICP OES. A multiplexed approach using experimental designs was applied for method optimization. The optimal conditions were using 4 mL of 8 mol L−1 HNO3 and 1.5 mL H2O2 under 30 min of sonication. The detectability of the method has been improved. The precision was RSD < 5.5% while the accuracy of the method ranged from 87% to 108% as well as the results were in agreement with the reference method. The analysis of 38 samples of Cajuína juices presented a mean of Ca, Cu, Fe, K, Mg, Na, P, S and Zn of 8.70, 0.10, 0.97, 1223, 112, 60.1, 83.9, 65.1, and 0.99 mg L−1. So, the proposed analytical method demonstrated feasibility for the simultaneous determination of mineral nutrients in similar matrices as beverage.
Thesagro:	Cajuína
Keywords:	Ultrasound-assisted extraction Factorial experimental design and response surface methodology ICP OES
DOI:	10.1016/j.focha.2023.100265
Type of Material:	Artigo de periódico
Access:	openAccess
Appears in Collections:	Artigo em periódico indexado (CPPSE)